Phase transitions like those seen in Ice XXI might seem mundane, but this was a cool find by scientists—literally. They did so for the first time through a pioneering X-ray laser technique. This extraordinary discovery, published in the journal Nature Materials, means that Ice XXI is stable even at room temperature. The implication of this finding is tremendous, creating thrilling new frontiers in materials science and planetary studies. The research team conducted their experiments at the European Synchrotron Radiation Facility. To make conditions required to find this new ice phase, they utilized the High Energy Density (HED) instrument from the European XFEL.
The researchers reached a remarkable high pressure of two gigapascals in just 10 milliseconds. The maximum compression rate was 120 gigapascals per second. This innovation made it possible for them to probe the fundamental nature of water, even under the most extreme conditions. To do this, they needed to study water under conditions of pressure nearly 20,000 times greater than normal atmospheric pressure. That deep investigation allowed them to crack the code on a new ice phase.
Understanding Ice XXI
Ice XXI is one of over 20 known crystalline forms of ice. These phases are numbered in Roman numerals, which may apply to other abundantly found ice forms such as ice I, ice II, and ice III. The existence of Ice XXI further expands our understanding of water’s complex solid state. It expands our awe and our understanding of the complexities at play. Ice XXI has astonishing properties which might advance the study of a number of scientific disciplines. This is the case for climatology, astrophysics, and materials science.
This new phase is especially significant because it exemplifies stability at room temperature. Underlying previous phases of ice were conditions that were extremely difficult to reproduce, rendering Ice XXI a remarkable outlier. Synthesizing and characterizing this stable phase at room temperature may open exploratory floodgates. Such insights can help us better understand how water acts across different environments on Earth, but in extraplanetary environments.
Methodology and Instruments Used
Inside the study, the researchers used cutting-edge technology to create the required conditions for Ice XXI to form. The High Energy Density (HED) instrument at the European XFEL was instrumental to this science. It created the high-pressure cooker climate necessary for the pre-innovative death matrix outcome. The researchers employed an anvil cell, which was released over a period of one second, to create the extreme pressures needed to facilitate the formation of the new ice phase.
By creating pressures of two gigapascals almost instantaneously, scientists were able to see how water molecules act when put under stress. This research represents a major advancement in our scientific understanding. In addition, it creates exciting new opportunities to study the fundamental physical properties of water and ice at extreme conditions.
Implications for Future Research
Uncovering Ice XXI is more than just an obvious new classification. It raises critical scientific questions about the state and properties of water in extreme environments and novel and unconventional conditions. Ice VI, another intriguing phase of ice believed to exist within icy moons such as Titan and Ganymede, raises questions about how these phases may influence geological and atmospheric processes on celestial bodies.
The European XFEL’s Water Call initiative has proven beneficial in advancing this line of research, fostering collaboration among scientists keen on exploring water’s various states. Expanding the scientific picture Researchers are exploring new phases such as Ice XXI. This finding allows them to know how water acts under extreme conditions across Earth and in outer space.

